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Molecular
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How
to Make Ethanol
Myths |
Making
Ethanol in the 25 Gallon VonHeltzen Still
The
following instructions are general guidelines. The details of
the process are dependant on so many variables that specific
instructions for every variable are not possible. Variables include:
the different sugar/starch based plants used to ferment, whether
those plants are dry or wet, the temperature and how long it
is sustained, the yeast and enzymes used, cleanliness. . . .
The variables will effect the time required and quantity of ethanol
produced in your batch. So these instructions will assume you
are using dried, cracked corn.
- Place
the 25 gallon pot on the stand and hook your propane tank to
the burner. Fill the pot with 20 gallons of water. Light the
burner and start heating the water.
- If you
are using batch processing there is a slight chance that the
corn will be tainted with bad bacteria, which can destroy the
yeast and stop the fermentation of ethanol. If you are concerned
about the cleanliness of your corn, boil the 20 gallons of
water. If you know your corn is clean, heat the water to about
200º.
For your safety, turn off the burner before you add the corn.
- Add 40lbs
of corn and let the mixture cool down.
- At 200º
or less add a little less than a tablespoon of the alpha-amylase
enzyme, stir.
- At 144º
or less add a little less than a tablespoon of the gluco-amylase
enzyme, stir.
- At 120º
or less add a little less than a tablespoon of the yeast, stir.
(Adding more enzymes or yeast than is required will not negatively affect
the batch.)
- Use the
hydrometer to monitor the percentage of alcohol in the liquid.
When the percentage of alcohol reaches 18% the yeast will die
and the fermentation will be over.
- Strain
the corn from the liquid. Leave the liquid in the pot, and
if you have livestock you can feed the corn to them. They will
love you for it.
- You will
now need a container of water, the size of a large kitchen
trash can or larger. Plug one of the smaller clear tubes onto
the pump and then onto the top pipe on the side of the condenser.
Plug the other small clear tube onto the lower pipe on the
side of the condenser and run it into the water container.
Plug the remaining larger clear tube onto the bottom pipe of
the condenser and run it into a container to collect the ethanol.
Put the pump into the water without getting the plug wet. Plug in the pump
and check the connections to verify that the water is pumping into the condenser
and out again into the water tank. Leave it on.
- Turn the
burner back on and heat the water/alcohol mixture until the
thermometer at the top of the column reads between 170º and
180º degrees. This will allow the ethanol to evaporate quickly
and enter the condenser, which will turn it back into a liquid.
The water/alcohol mixture will want stay around 170º to 180º
because of the ethanol. As the ethanol evaporates from the
water the temperature will easily rise too high.
- When the
liquid first comes out of the condenser it will contain a high
concentration of ethanol. As time passes the mixture will become
more diluted. It will be up to you to decide when to stop distillation.
(Do not discard the liquid left in the pot. You can use it for your next
batch.)
- Put your
molecular sieve into the pot with the ethanol and let it absorb
the excess water. Remove the sieve and heat it to remove the
water. If the sieve is cared for, it can be reused thousands
of times.
That’s
it, good luck.
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